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style="font-family:宋體">值至</span>10.5<span style="font-family:宋體">左右，混勻。放置使沉淀，用經(jīng)無(wú)氨水充分洗滌過(guò)的中速濾紙過(guò)濾，棄去初濾液</span>20ml.<span style="font-family:宋體">剩下的濾液按氨氮測定方法測定。</span></p><p>2<span style="font-family:宋體">、蒸餾法：分取</span>250ml<span style="font-family:宋體">水樣（如氨氮含量較高，可分取適量水樣加水至</span>250ml<span style="font-family:宋體">使氨氮含量不超過(guò)</span>2.5mg<span style="font-family:宋體">），移入凱氏燒瓶中，加數滴溴百里酚藍指示液，用氫氧化鈉或鹽酸溶液調</span>PH<span style="font-family:宋體">值</span>7<span style="font-family:宋體">左右。加入</span>0.25g<span style="font-family:宋體">輕質(zhì)氧化鎂和數粒玻璃珠，立即鏈接氮球和冷凝管，導管下端插入吸收液液面以下，吸收液為</span>50ml<span style="font-family:宋體">濃度為</span>20g/L<span style="font-family:宋體">的硼酸溶液，盛裝于</span>250ml<span style="font-family:宋體">錐形瓶中。加熱蒸餾，至餾出液達</span>200ml<span style="font-family:宋體">時(shí)停止蒸餾。定容至</span>250ml<span style="font-family:宋體">。再按氨氮測定方法測定。</span></p> </div> <div id="bd8lmiie" class="ly_PrevNext"> <ul> <li>上一篇：<a href="/Article-1395486.html">氨氮實(shí)驗如何調水樣的PH值？</a></li> <li>下一篇：<a 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